1YOD
Crystal structure of a water soluble analog of phospholamban
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-03-03 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9765, 0.9766, 0.9643 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 46.996, 46.996, 120.136 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 1.800 |
R-factor | 0.21176 |
Rwork | 0.209 |
R-free | 0.25724 |
Structure solution method | MAD |
RMSD bond length | 0.034 |
RMSD bond angle | 1.663 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.850 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.073 | 0.430 |
Number of reflections | 7658 | |
<I/σ(I)> | 13.1 | 2.8 |
Completeness [%] | 99.8 | 100 |
Redundancy | 18 | 18 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | 1,6 hexanediol, sodium citrate, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |