1YOC
Crystal Structure of genomics APC5556
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-BM |
Synchrotron site | APS |
Beamline | 19-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-10-06 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.97943 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 88.162, 113.399, 58.838 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.830 - 1.700 |
R-factor | 0.167 |
Rwork | 0.167 |
R-free | 0.20000 |
Structure solution method | Sulfur SAD |
RMSD bond length | 0.018 |
RMSD bond angle | 2.100 |
Data reduction software | DENZO |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.760 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.083 | 0.685 |
Number of reflections | 59643 | |
<I/σ(I)> | 7.5 | 2.47 |
Completeness [%] | 99.3 | 93.6 |
Redundancy | 9 | 8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | Na Formate, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |