1YNB
crystal structure of genomics APC5600
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 14-BM-D |
| Synchrotron site | APS |
| Beamline | 14-BM-D |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-10-30 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 1.00 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 85.320, 131.410, 58.560 |
| Unit cell angles | 90.00, 117.20, 90.00 |
Refinement procedure
| Resolution | 28.360 - 1.760 |
| R-factor | 0.206 |
| Rwork | 0.206 |
| R-free | 0.24300 |
| Structure solution method | Sulfur SAD |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.500 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | CNS (1.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.790 |
| High resolution limit [Å] | 1.760 | 1.760 |
| Rmerge | 0.039 | 0.039 |
| Number of reflections | 55813 | |
| <I/σ(I)> | 17 | 17 |
| Completeness [%] | 98.2 | 98.2 |
| Redundancy | 4.7 | 4.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 295 | Ammonium Sulphate, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 295K |
