1YN8
SH3 domain of yeast NBP2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | X11 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-11-29 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.8128 |
| Spacegroup name | P 1 |
| Unit cell lengths | 32.410, 53.300, 57.830 |
| Unit cell angles | 111.94, 90.98, 104.18 |
Refinement procedure
| Resolution | 20.000 - 1.700 |
| R-factor | 0.16677 |
| Rwork | 0.164 |
| R-free | 0.22434 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.394 |
| Data scaling software | XDS |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.800 |
| High resolution limit [Å] | 1.700 | 1.700 |
| Number of reflections | 36727 | |
| <I/σ(I)> | 7.9 | 2.8 |
| Completeness [%] | 96.5 | 95 |
| Redundancy | 2.3 | 2.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
