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1YLL

Crystal Structure of the Conserved Protein of Unknown Function PA5104 from Pseudomonas aeruginosa PAO1

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-ID
Synchrotron siteAPS
Beamline19-ID
Temperature [K]100
Detector technologyCCD
Collection date2004-12-21
DetectorADSC QUANTUM 315
Wavelength(s)0.9793, 0.9794, 0.956
Spacegroup nameP 1 21 1
Unit cell lengths68.514, 67.209, 82.768
Unit cell angles90.00, 111.35, 90.00
Refinement procedure
Resolution77.150 - 1.640
R-factor0.19906
Rwork0.194
R-free0.24328
Structure solution methodMAD
RMSD bond length0.010
RMSD bond angle1.763
Data scaling softwareHKL-2000
Phasing softwareSHARP
Refinement softwareREFMAC (5.2.0005)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]77.1501.700
High resolution limit [Å]1.6401.640
Rmerge0.0710.466
Number of reflections82845
<I/σ(I)>12.42.7
Completeness [%]88.7
Redundancy8.16.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8.5295PEG4000, magnesium chloride, Tris, L-lysine, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 295K

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