1YJO
Structure of NNQQNY from yeast prion Sup35 with zinc acetate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID13 |
Synchrotron site | ESRF |
Beamline | ID13 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-09-22 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 21.153, 4.870, 23.130 |
Unit cell angles | 90.00, 102.93, 90.00 |
Refinement procedure
Resolution | 22.540 - 1.300 |
R-factor | 0.103 |
Rwork | 0.102 |
R-free | 0.15200 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.077 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MLPHARE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 80.000 | 1.400 |
High resolution limit [Å] | 1.300 | 1.300 |
Number of reflections | 2166 | |
<I/σ(I)> | 9.8 | 2.6 |
Completeness [%] | 97.1 | 88.8 |
Redundancy | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 293 | ZINC SULFATE, SODIUM ACETATE, HEPES, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 293K, pH 7.00 |