1YJ7
Crystal structure of enteropathogenic E.coli (EPEC) type III secretion system protein EscJ
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-07-16 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.000 |
Spacegroup name | P 65 |
Unit cell lengths | 164.817, 164.817, 67.179 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.200 - 1.800 |
R-factor | 0.185 |
Rwork | 0.184 |
R-free | 0.20600 |
Structure solution method | SAD |
RMSD bond length | 0.013 |
RMSD bond angle | 1.232 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | REFMAC (5.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.170 | 1.890 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.082 | 0.313 |
Number of reflections | 96428 | |
<I/σ(I)> | 4.6 | |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 5.6 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8.2 | 291 | di-ammonium hydrogen phosphate, pH 8.2, VAPOR DIFFUSION, temperature 291K |
1 | VAPOR DIFFUSION | 8.2 | 291 | di-ammonium hydrogen phosphate, pH 8.2, VAPOR DIFFUSION, temperature 291K |