1YH3
Crystal structure of human CD38 extracellular domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-07-20 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.916 |
Spacegroup name | P 1 |
Unit cell lengths | 41.839, 51.491, 66.439 |
Unit cell angles | 108.27, 90.47, 97.29 |
Refinement procedure
Resolution | 10.000 - 1.910 |
R-factor | 0.19174 |
Rwork | 0.188 |
R-free | 0.25336 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.029 |
RMSD bond angle | 2.264 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.930 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 40203 | |
Completeness [%] | 97.9 | 94.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 297 | MES, PEG4000, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 297K |