1YGE
LIPOXYGENASE-1 (SOYBEAN) AT 100K
Experimental procedure
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1993-04 |
Detector | MAC Science DIP-2000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 94.900, 94.000, 49.900 |
Unit cell angles | 90.00, 90.10, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.400 |
R-factor | 0.197 |
Rwork | 0.197 |
R-free | 0.24300 |
RMSD bond length | 0.011 * |
RMSD bond angle | 1.700 * |
Data reduction software | HKL ((DENZO)) |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 * | |
High resolution limit [Å] | 1.400 * | 1.400 * |
Rmerge | 0.067 | |
Number of reflections | 161029 | |
Completeness [%] | 96.0 | 92 * |
Redundancy | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 5.6 * | 21 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | acetate | 0.1 (M) | |
2 | 1 | drop | PEG3400 | 4 (%(w/v)) | |
3 | 1 | drop | enzyme | 4-5 (mg/ml) | |
4 | 1 | reservoir | PEG3400 | 8 (%(w/v)) |