1YG6
ClpP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X25 |
| Synchrotron site | NSLS |
| Beamline | X25 |
| Temperature [K] | 99 |
| Detector technology | CCD |
| Collection date | 2002-06-06 |
| Detector | BRANDEIS - B4 |
| Wavelength(s) | 0.98 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 192.500, 103.300, 159.000 |
| Unit cell angles | 90.00, 98.40, 90.00 |
Refinement procedure
| Resolution | 30.000 - 1.900 |
| R-factor | 0.228 |
| Rwork | 0.221 |
| R-free | 0.25100 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | RESIDUES 20-193 1tys.PDB |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.800 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 1.850 |
| Rmerge | 0.088 |
| Number of reflections | 247428 |
| <I/σ(I)> | 30 |
| Completeness [%] | 95.9 |
| Redundancy | 5.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.2 | 298 | mpd, mes, pH 6.2, VAPOR DIFFUSION, SITTING DROP, temperature 298K |
