1YFS
The crystal structure of alanyl-tRNA synthetase in complex with L-alanine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 173.026, 73.868, 73.999 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.080 |
R-factor | 0.2 |
Rwork | 0.189 |
R-free | 0.23600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1riq |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.080 |
Number of reflections | 57744 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.2 | 298 | PEG 5000 mme, NaCl, Tris-Cl, Tris-base, L-alanine, pH 6.2, VAPOR DIFFUSION, SITTING DROP, temperature 298K |