1YE3
HORSE LIVER ALCOHOL DEHYDROGENASE APOENZYME
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-07-23 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.000 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 55.780, 74.290, 181.250 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.200 - 1.590 |
R-factor | 0.2011 |
Rwork | 0.199 |
R-free | 0.25593 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 8adh |
RMSD bond length | 0.014 |
RMSD bond angle | 1.529 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.200 | 1.650 |
High resolution limit [Å] | 1.590 | 1.590 |
Rmerge | 0.075 | 0.211 |
Number of reflections | 36732 | |
<I/σ(I)> | 11.5 | 4.7 |
Completeness [%] | 71.9 | 58 |
Redundancy | 5.66 | 5.74 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICRODIALYSIS | 8.4 | 278 | 50 mM Tris-HCl, 25% methylpentanediol, pH 8.4, MICRODIALYSIS, temperature 278K |