1YAI
X-RAY STRUCTURE OF A BACTERIAL COPPER,ZINC SUPEROXIDE DISMUTASE
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 293 |
Detector technology | AREA DETECTOR |
Collection date | 1991-07-20 |
Detector | SIEMENS |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 120.700, 87.000, 43.500 |
Unit cell angles | 90.00, 90.60, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.900 |
R-factor | 0.149 * |
Rwork | 0.149 |
R-free | 0.21000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3sod |
RMSD bond length | 0.013 |
RMSD bond angle | 17.802 * |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | AMoRE |
Refinement software | TNT (5E) |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.900 |
Rmerge | 0.049 * |
Total number of observations | 116490 * |
Number of reflections | 30277 * |
Completeness [%] | 83.0 |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 6.5 | 20 * | macroseeding * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 20 (mg/ml) | |
2 | 1 | drop | potassium phosphate | 60 (mM) | |
3 | 1 | reservoir | MPD | 42 (%) | |
4 | 1 | reservoir | potassium phosphate | 60 (mM) |