1Y8J
Crystal Structure of human NEP complexed with an imidazo[4,5-c]pyridine inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS FR591 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2003-08-13 |
Detector | MARRESEARCH |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 107.355, 107.356, 112.466 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 2.250 |
R-factor | 0.22984 |
Rwork | 0.226 |
R-free | 0.29637 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1dmt |
RMSD bond length | 0.007 |
RMSD bond angle | 0.889 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.390 |
High resolution limit [Å] | 2.250 | 2.250 |
Number of reflections | 34323 | |
Completeness [%] | 95.4 | 84.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | VAPOR DIFFUSION, HANGING DROP |