1Y6I
Synechocystis GUN4
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | MACSCIENCE |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2003-06-15 |
| Detector | MACSCIENCE DIP100 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 63.907, 70.710, 72.645 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 32.310 - 1.780 |
| R-factor | 0.221 |
| Rwork | 0.221 |
| R-free | 0.25900 |
| Structure solution method | MIR |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.800 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.000 | |
| High resolution limit [Å] | 1.780 | 1.780 |
| Number of reflections | 17157 | |
| <I/σ(I)> | 15.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | PEG 8000, NaBr, DTT, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
