1Y21Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU300 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2002-08-01 |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 48.065, 41.477, 65.346 |
| Unit cell angles | 90.00, 94.55, 90.00 |
Refinement procedure
| Resolution | 64.550 - 1.750 |
| R-factor | 0.1696 |
| Rwork | 0.168 |
| R-free | 0.20828 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | 1ntf |
| RMSD bond length | 0.023 |
| RMSD bond angle | 1.831 |
| Data reduction software | d*TREK |
| Data scaling software | d*TREK |
| Phasing software | MLPHARE |
| Refinement software | REFMAC (5.1.22) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 64.550 | 1.810 |
| High resolution limit [Å] | 1.750 | 1.750 |
| Number of reflections | 24549 | |
| <I/σ(I)> | 20 | 2.6 |
| Completeness [%] | 98.7 | 98.4 |
| Redundancy | 3.3 | 2.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.6 | 298 | PEG 4000, pH 8.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
