1XZ2
wild-type hemoglobin deoxy no-salt
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 298 |
Detector technology | AREA DETECTOR |
Collection date | 1994-03-07 |
Detector | SDMS |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 83.900, 112.100, 63.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.900 |
R-factor | 0.17136 |
Rwork | 0.168 |
R-free | 0.20094 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1hbb |
RMSD bond length | 0.014 |
RMSD bond angle | 1.491 |
Data reduction software | SDMS |
Data scaling software | SDMS |
Phasing software | X-PLOR |
Refinement software | REFMAC (5.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.070 |
High resolution limit [Å] | 1.930 | 1.930 |
Rmerge | 0.059 | 0.185 |
Number of reflections | 44690 | |
<I/σ(I)> | 12.4 | 2.9 |
Completeness [%] | 96.6 | 83.2 |
Redundancy | 9 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | batch | 7 | 298 | 12% PEG 1450, 10 mg/ml Hb, pH 7.0, batch, temperature 298.0K |