1XYM
THE ROLE OF THE DIVALENT METAL ION IN SUGAR BINDING, RING OPENING, AND ISOMERIZATION BY D-XYLOSE ISOMERASE: REPLACEMENT OF A CATALYTIC METAL BY AN AMINO-ACID
Experimental procedure
Spacegroup name | P 21 21 2 |
Unit cell lengths | 88.120, 99.530, 94.790 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.800 |
R-factor | 0.197 |
Rwork | 0.197 |
RMSD bond length | 0.015 |
RMSD bond angle | 2.686 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.800 * |
Number of reflections | 57060 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 7.5 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium sulfate | 45 (%sat) | |
2 | 1 | drop | enzyme | 43 (mg/ml) | |
3 | 1 | drop | PIPES | 43 (mg/ml) | |
4 | 1 | drop | 0.010 (M) | ||
5 | 1 | drop | 0.001 (M) |