1XWO
crystal structrue of goose delta crystallin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2003-10-10 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.542 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 93.700, 99.000, 106.500 |
Unit cell angles | 90.00, 101.40, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.800 |
R-factor | 0.22 |
Rwork | 0.210 |
R-free | 0.28900 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.300 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.850 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.145 | |
Number of reflections | 45763 | |
Completeness [%] | 99.7 | 99.1 |
Redundancy | 16.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | PEG 2000, magnesium chloride, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |