1XVX
Crystal Structure of iron-loaded Yersinia enterocolitica YfuA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2004-07-13 |
| Detector | RIGAKU |
| Wavelength(s) | 1.5418 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 108.392, 46.951, 62.454 |
| Unit cell angles | 90.00, 103.51, 90.00 |
Refinement procedure
| Resolution | 60.860 - 1.530 |
| R-factor | 0.16304 |
| Rwork | 0.161 |
| R-free | 0.19304 |
| Structure solution method | SAD |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.221 |
| Data reduction software | d*TREK |
| Data scaling software | CCP4 ((TRUNCATE)) |
| Phasing software | SHELXD |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 33.560 | 1.580 |
| High resolution limit [Å] | 1.530 | 1.530 |
| Number of reflections | 35434 | |
| Completeness [%] | 80.6 | 11.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | zinc acetate dihydrate, PEG 8000, sodium cacodylate, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
