1XUI
TRYPSIN-KETO-BABIM, ZN+2-FREE, PH 8.2
Experimental procedure
Detector technology | IMAGE PLATE |
Detector | RIGAKU |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 54.960, 54.960, 109.120 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 7.500 * - 1.500 |
R-factor | 0.198 * |
Rwork | 0.192 |
R-free | 0.22300 |
RMSD bond length | 0.018 |
RMSD bond angle | 26.800 * |
Data reduction software | bioteX ((MSC)) |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 1.570 | |
High resolution limit [Å] | 1.500 | |
Rmerge | 0.067 | |
Total number of observations | 69702 * | |
Number of reflections | 69702 | |
Completeness [%] | 71.9 | 32.2 |
Redundancy | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 8.2 | CRYSTALLIZED IN ABSENCE OF ZN+2, WITH MOTHER LIQUOR SATURATED IN KETO-BABIM., pH 8.2 |