1XUC

Matrix metalloproteinase-13 complexed with non-zinc binding inhibitor

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-1
Synchrotron site	ESRF
Beamline	ID14-1
Temperature [K]	100
Detector technology	CCD
Detector	ADSC QUANTUM 4
Wavelength(s)	0.934
Spacegroup name	C 1 2 1
Unit cell lengths	134.437, 36.476, 95.320
Unit cell angles	90.00, 130.51, 90.00

Refinement procedure

Resolution	50.000 - 1.700
Rwork	0.175
R-free	0.20000
Structure solution method	MOLECULAR REPLACEMENT
Data scaling software	XDS
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.800
High resolution limit [Å]	1.700	1.700
Number of reflections	38478
<I/σ(I)>	14.74	8.2
Completeness [%]	97.8	90.5
Redundancy	3.5	2.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1