1XT9
Crystal Structure of Den1 in complex with Nedd8
Experimental procedure
Experimental method | SIR |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-10-22 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9790 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 68.849, 71.626, 52.947 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.620 - 2.200 |
R-factor | 0.209 |
Rwork | 0.209 |
R-free | 0.25900 |
Structure solution method | SIR |
RMSD bond length | 0.010 |
RMSD bond angle | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.170 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.087 | 0.250 |
Number of reflections | 22541 | |
<I/σ(I)> | 12.5 | 1.86 |
Completeness [%] | 90.2 | 85.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9 | 291 | 2M ammonium sulfate, 0.1M bicine, 4% tert-butanol, pH 9.0, VAPOR DIFFUSION, HANGING DROP, temperature 291K |