1XSZ
The structure of RalF
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X26C |
| Synchrotron site | NSLS |
| Beamline | X26C |
| Temperature [K] | 108 |
| Detector technology | CCD |
| Collection date | 2003-08-27 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.9795 |
| Spacegroup name | P 31 |
| Unit cell lengths | 84.559, 84.559, 110.175 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 40.000 - 1.410 |
| Rwork | 0.202 |
| R-free | 0.22510 |
| Structure solution method | MIR |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.200 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.000 | 1.450 |
| High resolution limit [Å] | 1.410 | 1.410 |
| Rmerge | 0.044 | 0.368 |
| Number of reflections | 171080 | |
| <I/σ(I)> | 27.4 | 2.5 |
| Completeness [%] | 99.5 | 99.7 |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 294 | sodium formate, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 294K |
