1XQB
X-Ray Structure Of YaeB from Haemophilus influenzae. Northeast Structural Genomics Research Consortium (NESGC)target IR47.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X4A |
| Synchrotron site | NSLS |
| Beamline | X4A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 69.650, 69.914, 119.833 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.740 - 2.850 |
| R-factor | 0.279 |
| Rwork | 0.279 |
| R-free | 0.32400 |
| Structure solution method | SAD |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.400 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.950 |
| High resolution limit [Å] | 2.850 | 2.850 |
| Rmerge | 0.068 | 0.370 |
| Number of reflections | 13232 | |
| <I/σ(I)> | 18.927 | |
| Completeness [%] | 99.5 | 100 |
| Redundancy | 5.48 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.6 | 294 | 1.2 M ammonium sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 294K, pH 5.60 |
