1XPQ
Crystal structure of fms1, a polyamine oxidase from yeast
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE A1 |
| Synchrotron site | CHESS |
| Beamline | A1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-08-06 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.94740 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 103.048, 98.133, 123.832 |
| Unit cell angles | 90.00, 103.28, 90.00 |
Refinement procedure
| Resolution | 42.930 - 2.510 |
| R-factor | 0.202 |
| Rwork | 0.200 |
| R-free | 0.27610 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.500 |
| Number of reflections | 66331 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 296 | 10% PEG 4000, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 296K |
