1XOG

N9 Tern Influenza neuraminidase complexed with a 2,5-Disubstituted tetrahydrofuran-5-carboxylic acid

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	100
Detector technology	IMAGE PLATE
Detector	RIGAKU RAXIS
Wavelength(s)	1.54
Spacegroup name	I 4 3 2
Unit cell lengths	180.344, 180.344, 180.344
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	9.990 - 2.800
Rwork	0.221
R-free	0.29700
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.008
RMSD bond angle	1.500
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNX (2000)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	10.000	2.980
High resolution limit [Å]	2.800	2.800
Number of reflections	12672
Completeness [%]	92.8	84.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1