1XOD
Crystal structure of X. tropicalis Spred1 EVH-1 domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX14.2 |
Synchrotron site | SRS |
Beamline | PX14.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-05-22 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.975 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 32.811, 38.193, 79.907 |
Unit cell angles | 90.00, 95.68, 90.00 |
Refinement procedure
Resolution | 79.060 - 1.150 |
R-factor | 0.15538 |
Rwork | 0.154 |
R-free | 0.17700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | pdb entries 1EVH 1i7a 1qc6 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.335 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 79.000 | 1.170 |
High resolution limit [Å] | 1.150 | 1.150 |
Number of reflections | 68977 | |
<I/σ(I)> | 19.4 | 3.99 |
Completeness [%] | 97.7 | 94.5 |
Redundancy | 3.9 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 298 | PEG 3350, potassium fluoride, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |