1XGF
Backbone Structure of COCOSIN, an 11S storage protein from cocos nucifera
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 293 |
| Detector technology | IMAGE PLATE |
| Collection date | 2002-01-10 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.5418 |
| Spacegroup name | H 3 |
| Unit cell lengths | 93.659, 93.659, 216.450 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 2.800 - 2.610 |
| R-factor | 0.2401 |
| Rwork | 0.240 |
| R-free | 0.29440 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1od5 |
| Data reduction software | AUTOMAR |
| Phasing software | AMoRE |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.800 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Number of reflections | 21429 | |
| Completeness [%] | 99.8 | 93.78 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.7 | 293 | 20% MPD, Na/K Phosphate buffer containing 7% NaCl, pH 6.7, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
