1XDH
Structure of plasmepsin II in complex with pepstatin A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 141.111, 141.111, 97.102 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 119.520 - 1.700 |
R-factor | 0.21545 |
Rwork | 0.214 |
R-free | 0.23712 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.276 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | MOLREP |
Refinement software | REFMAC (5.1.24) |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |