1XD6
Crystal structures of novel monomeric monocot mannose-binding lectins from Gastrodia elata
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6B |
Synchrotron site | Photon Factory |
Beamline | BL-6B |
Temperature [K] | 298 |
Detector technology | DIFFRACTOMETER |
Collection date | 2001-04-15 |
Detector | WEISSENBERG |
Wavelength(s) | 0.98 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 78.070, 97.480, 36.120 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 18.930 - 2.000 |
R-factor | 0.20267 |
Rwork | 0.199 |
R-free | 0.23829 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.297 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 18.930 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 9217 | |
<I/σ(I)> | 7.1 | |
Completeness [%] | 95.5 | 91.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | ammonium sulfate, MPD, MES, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277.0K |