1XAN
HUMAN GLUTATHIONE REDUCTASE IN COMPLEX WITH A XANTHENE INHIBITOR
Experimental procedure
Spacegroup name | C 1 2 1 |
Unit cell lengths | 119.790, 63.350, 84.650 |
Unit cell angles | 90.00, 58.61, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.000 |
R-factor | 0.158 |
Rwork | 0.158 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.000 * |
Rmerge | 0.071 * |
Number of reflections | 33736 * |
Completeness [%] | 92.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | hGR | 20 (mg/ml) | |
2 | 1 | drop | ammonium sulfate | 3 (%) | |
3 | 1 | drop | potassium phosphate | 0.1 (M) | |
4 | 1 | drop | beta-octylglucoside | 0.1 (%) | |
5 | 1 | reservoir | ammonium sulfate | 21-23 (%) | |
6 | 1 | reservoir | potassium phosphate | 0.1 (M) |