1X81

Farnesyl transferase structure of Jansen compound

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Wavelength(s)	1.00000
Spacegroup name	P 61
格子定数 [Å]	170.086, 170.086, 69.133
格子定数 [度]	90.00, 90.00, 120.00

精密化法

残基	50.000 - 3.500
Rwork	0.223
R-free	0.29200
Structure solution method	FOURIER SYNTHESIS
結合長の平均二乗偏差(RMSD) [Å]	0.011
結合角の平均二乗偏差(RMSD) [度]	1.700
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	X-PLOR
Refinement software	X-PLOR (98.0)

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)	50.000	3.720
分解能 [Å] (高)	3.500	3.500
独立反射数	13627
完全性 [%]	93.2	92

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	VAPOR DIFFUSION, HANGING DROP	4.5		pH 4.5, VAPOR DIFFUSION, HANGING DROP