1X25
Crystal Structure of a Member of YjgF Family from Sulfolobus Tokodaii (ST0811)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2004-09-01 |
Detector | RIGAKU RAXIS VII |
Wavelength(s) | 1.5418 |
Spacegroup name | H 3 |
Unit cell lengths | 54.980, 54.980, 221.557 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.030 - 2.000 |
R-factor | 0.14787 |
Rwork | 0.146 |
R-free | 0.18799 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1qd9 |
RMSD bond length | 0.020 |
RMSD bond angle | 1.488 |
Data reduction software | CrystalClear ((MSC/RIGAKU)) |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | MOLREP |
Refinement software | REFMAC (5.1.19) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 22.051 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.061 | 0.151 |
Number of reflections | 16882 | |
<I/σ(I)> | 9.8 | 5.1 |
Completeness [%] | 99.8 | 99.8 |
Redundancy | 6.2 | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.3 | 293 | PEG 10000, Bis-Tris, ammonium acetate, pH 5.3, VAPOR DIFFUSION, SITTING DROP, temperature 293K |