1X1Z

Orotidine 5'-monophosphate decarboxylase (odcase) complexed with BMP (produced from 6-cyanoump)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 14-ID-B
Synchrotron site	APS
Beamline	14-ID-B
Temperature [K]	100
Detector technology	CCD
Collection date	2003-02-22
Detector	MARRESEARCH
Wavelength(s)	0.9755
Spacegroup name	P 1 21 1
Unit cell lengths	58.105, 73.568, 59.399
Unit cell angles	90.00, 119.28, 90.00

Refinement procedure

Resolution	17.620 - 1.450
R-factor	0.162
Rwork	0.162
R-free	0.18000
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.015
RMSD bond angle	1.600
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNS (1.1)

Data quality characteristics

	Overall
Low resolution limit [Å]	100.000
High resolution limit [Å]	1.450
Number of reflections	77021
Completeness [%]	100.0

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	293	SODIUM CITRATE, MES, DIOXANE, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K