1WW7
Agrocybe cylindracea galectin (Ligand-free)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | MACSCIENCE |
Temperature [K] | 293 |
Detector technology | AREA DETECTOR |
Collection date | 1999-02-10 |
Detector | SIEMENS HI-STAR |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 57.071, 96.307, 121.656 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.900 |
R-factor | 0.203 |
Rwork | 0.203 |
R-free | 0.25200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.300 |
Data reduction software | SADIE |
Data scaling software | SAINT |
Phasing software | CNS |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.700 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 51284 | |
<I/σ(I)> | 11.09 | 1.86 |
Completeness [%] | 95.4 | 85.9 |
Redundancy | 5.32 | 2.95 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.1 | 293 | ammomium sulfate, pipes, pH 7.1, VAPOR DIFFUSION, HANGING DROP, temperature 293K |