1WVH
Crystal structure of tensin1 PTB domain
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-03-04 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.979, 0.9793, 0.8731 |
Spacegroup name | I 4 |
Unit cell lengths | 75.680, 75.680, 48.690 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.500 |
R-factor | 0.218 |
Rwork | 0.218 |
R-free | 0.23600 |
Structure solution method | MAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.700 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.590 |
High resolution limit [Å] | 1.500 | 1.500 |
Number of reflections | 22134 | |
Completeness [%] | 99.9 | 99.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9.5 | 277 | PEG 600, CHES, pH 9.5, VAPOR DIFFUSION, SITTING DROP, temperature 277K |