1WUE
Crystal structure of protein GI:29375081, unknown member of enolase superfamily from enterococcus faecalis V583
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X9A |
| Synchrotron site | NSLS |
| Beamline | X9A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-09-21 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.97934, 0.97911, 0.97166 |
| Spacegroup name | H 3 |
| Unit cell lengths | 136.807, 136.807, 112.771 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 25.000 - 2.100 |
| R-factor | 0.211 |
| Rwork | 0.207 |
| R-free | 0.24200 |
| Structure solution method | MAD |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.420 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | CNS (1.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 25.000 | 2.180 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Number of reflections | 45287 | |
| Completeness [%] | 98.6 | 97.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6.5 | 293 | PEG 3350, Bis Tris, Sodium Chloride, pH 6.5, VAPOR DIFFUSION, temperature 293.0K |
