Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site | Photon Factory |
Beamline | BL-6A |
Detector technology | DIFFRACTOMETER |
Collection date | 1993-12-07 |
Detector | WEISSENBERG |
Wavelength(s) | 1.04 |
Spacegroup name | P 65 |
Unit cell lengths | 71.400, 71.400, 79.600 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 7.950 - 2.150 |
R-factor | 0.1973 |
Rwork | 0.192 |
R-free | 0.24731 |
Structure solution method | MIR |
RMSD bond length | 0.012 |
RMSD bond angle | 1.375 |
Data reduction software | WEIS |
Data scaling software | SCALE |
Phasing software | PROTEIN (SYSTEM (PROF. Y. MITSUI)) |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 10.000 | 1.880 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.048 | |
Number of reflections | 14666 | |
Completeness [%] | 66.2 | 12.9 |
Redundancy | 4.18 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.3 | 288 | Ammonium Sulfate, dioxane, acetate buffer, pH 5.3, VAPOR DIFFUSION, HANGING DROP, temperature 288K |