1WTN
The structure of HEW Lysozyme Orthorhombic Crystal Growth under a High Magnetic Field
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-18B |
| Synchrotron site | Photon Factory |
| Beamline | BL-18B |
| Temperature [K] | 296 |
| Detector technology | DIFFRACTOMETER |
| Collection date | 1999-06-21 |
| Detector | WEISSENBERG |
| Wavelength(s) | 1.0000 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 56.540, 73.830, 30.500 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 16.000 - 1.130 |
| Rwork | 0.170 |
| R-free | 0.20000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.018 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | EPMR |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.160 |
| High resolution limit [Å] | 1.130 | 1.130 |
| Number of reflections | 34449 | |
| Completeness [%] | 99.5 | 71.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | under a High Magnetic Field of 10T | 4.5 | 313 | NaCl, sodium acetate, pH 4.5, under a High Magnetic Field of 10T, temperature 313K |
| 1 | under a High Magnetic Field of 10T | 4.5 | 313 | NaCl, sodium acetate, pH 4.5, under a High Magnetic Field of 10T, temperature 313K |
