1WTM
X-ray structure of HEW Lysozyme Orthorhombic Crystal formed in the Earth's magnetic field
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-18B |
| Synchrotron site | Photon Factory |
| Beamline | BL-18B |
| Temperature [K] | 296 |
| Detector technology | DIFFRACTOMETER |
| Collection date | 1999-06-20 |
| Detector | WEISSENBERG |
| Wavelength(s) | 1.0000 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 56.440, 73.730, 30.430 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 16.000 - 1.330 |
| Rwork | 0.173 |
| R-free | 0.20100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.022 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | EPMR |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.380 |
| High resolution limit [Å] | 1.330 | 1.330 |
| Number of reflections | 20095 | |
| Completeness [%] | 93.6 | 62.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | in the Earth's magnetic field | 4.5 | 313 | NaCl, sodium acetate, pH 4.5, in the Earth's magnetic field, temperature 313K |
| 1 | in the Earth's magnetic field | 4.5 | 313 | NaCl, sodium acetate, pH 4.5, in the Earth's magnetic field, temperature 313K |
