1WS3
Urate oxidase from aspergillus flavus complexed with uracil
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | LURE BEAMLINE DW32 |
Synchrotron site | LURE |
Beamline | DW32 |
Temperature [K] | 291 |
Detector technology | IMAGE PLATE |
Collection date | 2003-10-09 |
Detector | MARRESEARCH |
Wavelength(s) | 0.972 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 140.601, 140.601, 151.076 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 15.000 - 3.200 |
Rwork | 0.146 |
R-free | 0.20000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1r51 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.230 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | BUSTER-TNT |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 36.000 |
High resolution limit [Å] | 3.200 |
Number of reflections | 28902 |
<I/σ(I)> | 13.3 |
Completeness [%] | 99.8 |
Redundancy | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 291 | pH 8.00, VAPOR DIFFUSION, SITTING DROP, temperature 291K |