1WRI
Crystal Structure of Ferredoxin isoform II from E. arvense
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2002-12-18 |
Detector | MACSCIENCE |
Wavelength(s) | 0.9 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 97.544, 29.411, 32.561 |
Unit cell angles | 90.00, 103.94, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.200 |
R-factor | 0.1184 |
Rwork | 0.109 |
R-free | 0.14070 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 0.033 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | CNS |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 16.500 | 1.240 |
High resolution limit [Å] | 1.200 | 1.200 |
Rmerge | 0.077 | |
Number of reflections | 27366 | |
<I/σ(I)> | 5.3 | |
Completeness [%] | 97.2 | 97.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 298 | Potassium phosphate, pH 7.5, VAPOR DIFFUSION, temperature 298K |