1WPR
Crystal structure of RsbQ inhibited by PMSF
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL38B1 |
Synchrotron site | SPring-8 |
Beamline | BL38B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-11-27 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 77.202, 80.999, 136.934 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.860 - 2.600 |
R-factor | 0.234 |
Rwork | 0.231 |
R-free | 0.29200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.500 |
Data reduction software | CrystalClear ((MSC/RIGAKU)) |
Data scaling software | CrystalClear ((MSC/RIGAKU)) |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.860 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 26989 | |
Completeness [%] | 99.5 | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | sodium malonate, VAPOR DIFFUSION, HANGING DROP, temperature 298K |