1WMP
Crystal structure of amine oxidase complexed with cobalt ion
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-11-08 |
Detector | Bruker DIP-6040 |
Wavelength(s) | 0.9 |
Spacegroup name | I 1 2 1 |
Unit cell lengths | 157.580, 63.376, 184.204 |
Unit cell angles | 90.00, 112.47, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.000 |
R-factor | 0.19 |
Rwork | 0.188 |
R-free | 0.22000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.300 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.087 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.094 | |
Number of reflections | 112241 | |
Completeness [%] | 98.8 | 98.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICRODIALYSIS | 6.8 | 289 | 1.05M POTASSIUM SODIUM TARTRATE, 25mM HEPES, pH 6.8, MICRODIALYSIS, temperature 289K |