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1WMP

Crystal structure of amine oxidase complexed with cobalt ion

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL44XU
Synchrotron siteSPring-8
BeamlineBL44XU
Temperature [K]100
Detector technologyCCD
Collection date2002-11-08
DetectorBruker DIP-6040
Wavelength(s)0.9
Spacegroup nameI 1 2 1
Unit cell lengths157.580, 63.376, 184.204
Unit cell angles90.00, 112.47, 90.00
Refinement procedure
Resolution10.000 - 2.000
R-factor0.19
Rwork0.188
R-free0.22000
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.006
RMSD bond angle1.300
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareX-PLOR
Refinement softwareX-PLOR (3.851)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]24.0872.110
High resolution limit [Å]2.0002.000
Rmerge0.094
Number of reflections112241
Completeness [%]98.898.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1MICRODIALYSIS6.82891.05M POTASSIUM SODIUM TARTRATE, 25mM HEPES, pH 6.8, MICRODIALYSIS, temperature 289K

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