1WMN
Crystal structure of topaquinone-containing amine oxidase activated by cobalt ion
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44B2 |
Synchrotron site | SPring-8 |
Beamline | BL44B2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1999-10-04 |
Detector | MARRESEARCH |
Wavelength(s) | 0.7 |
Spacegroup name | I 1 2 1 |
Unit cell lengths | 157.682, 63.094, 184.091 |
Unit cell angles | 90.00, 111.76, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.800 |
R-factor | 0.226 |
Rwork | 0.224 |
R-free | 0.27000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.810 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.078 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.061 | |
Number of reflections | 184098 | |
Completeness [%] | 99.7 | 99.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICRODIALYSIS | 6.8 | 289 | 1.05M POTASSIUM SODIUM TARTRATE, 25mM HEPES , pH 6.8, MICRODIALYSIS, temperature 289K |