1WMG
Crystal structure of the UNC5H2 death domain
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL26B1 |
Synchrotron site | SPring-8 |
Beamline | BL26B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-04-06 |
Detector | RIGAKU JUPITER |
Wavelength(s) | 0.979006, 0.979363, 0.964000 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 124.878, 47.207, 121.177 |
Unit cell angles | 90.00, 119.56, 90.00 |
Refinement procedure
Resolution | 39.780 - 2.100 |
R-factor | 0.229 |
Rwork | 0.229 |
R-free | 0.26900 |
Structure solution method | MAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.200 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 71778 | |
Completeness [%] | 99.6 | 99.2 |
Redundancy | 3.59 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIQUID DIFFUSION | 6.5 | 285 | MES, magnesium sulfate, pH 6.5, LIQUID DIFFUSION, temperature 285K |