1WK4
Crystal structure of ttk003001606
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL26B1 |
Synchrotron site | SPring-8 |
Beamline | BL26B1 |
Detector technology | CCD |
Collection date | 2004-04-11 |
Wavelength(s) | 0.96500, 0.97897, 0.97933 |
Spacegroup name | P 64 |
Unit cell lengths | 78.332, 78.332, 197.038 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.190 - 2.800 |
R-factor | 0.217 |
Rwork | 0.217 |
R-free | 0.27500 |
Structure solution method | MAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.200 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 33433 | |
<I/σ(I)> | 30.7 | 2.1 |
Completeness [%] | 99.9 | 100 |
Redundancy | 16.8 | 17.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | MES, sodium formate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 293.0K |