1WGI

STRUCTURE OF INORGANIC PYROPHOSPHATASE

Experimental procedure

Detector technology	IMAGE PLATE
Detector	RIGAKU
Spacegroup name	P 21 21 21
Unit cell lengths	54.300, 68.400, 161.900
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.200
R-factor	0.172
Rwork	0.172
R-free	0.21100
RMSD bond length	0.010
RMSD bond angle	25.000 *
Data reduction software	DENZO
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	8.000 *
High resolution limit [Å]	2.200 *	2.200 *
Rmerge	0.088
Total number of observations	178216 *
Number of reflections	27467 *
Completeness [%]	89.5 *	71.9 *
Redundancy	6.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1