1WD7
Crystal Structure of Uroporphyrinogen III Synthase from an Extremely Thermophilic Bacterium Thermus thermophilus HB8 (Wild type, Native, Form-2 crystal)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-03-07 |
Detector | Bruker DIP-6040 |
Wavelength(s) | 0.90000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 37.900, 84.875, 73.948 |
Unit cell angles | 90.00, 91.25, 90.00 |
Refinement procedure
Resolution | 37.890 - 1.600 |
R-factor | 0.224 |
Rwork | 0.224 |
R-free | 0.25500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1wcw |
RMSD bond length | 0.015 |
RMSD bond angle | 1.800 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | CNS (1.1) |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |